Specifications

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Question 1

The term craquelure itself refers to the crevices and cracks that form on the surface of the glaze. The pattern of these cracks is often circular, although they may be scattered across the surface of the glaze. The reason for the appearance of craquelure is either a difference in the coefficient of thermal expansion of the shard and the glaze, or deformation of the tile due to the impact of mechanical load on it.

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When craquelure appears on polished ceramic tiles and slabs, the term "polished craquelure" is used.

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The test method for determining the resistance to cracking of glazes (craquelure) of ceramic tiles and slabs is given in the EN ISO 10545-18 standard. To determine the resistance to cracking of glazes, tiles and slabs are subjected to high pressure steam in an autoclave. Then the tiles and slabs, after applying the dye to the glazed surfaces, are examined for the presence of cracks in the glaze.

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“Late craquelure” occurs under the influence of the external environment during operation. The reasons for its appearance are: thermal shock, insufficient drying of the cement base, excessive cement content in the layer, excessive thickness of the mortar layer.

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Glazed tiles with an "immediate crackle effect" are not considered defective, although manufacturers sometimes deliberately create collections of tiles with a "craquelure effect" for aesthetic purposes.

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This defect can appear immediately after the end of the production cycle (in this case they speak of “immediate craquelure”) or some time after laying the tiles (in this case they speak of “late craquelure”).

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The material on this issue is presented in the article “ Resistance to craquelure ” and “ Cracking of craquelure glaze ”.

Question 2

Slip resistance is determined by the kinetic and dynamic conditions of motion of the body interacting with the surface. When it comes to flooring, it is obvious how the degree of slip is related to the safety of using the surface. Knowledge of surface properties is essential for the cladding designer, tiler, retailer and end user, as well as the safety inspector. Please mark the correct conclusions in your opinion:

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The DIN 51130 and DIN 51097 methods, also called "incline plane methods", consist of a person walking back and forth on a platform covered with the tiles being tested. The inclination of the test section increases at a constant rate until an angle is reached at which the person begins to feel unsure when walking, that is, begins to slide.

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Ceramic tiles, characterized by their smoothness and shine, form the most intimate contact between the surface and the sole, thereby increasing the coefficient of friction. While rough, uneven surfaces tend to allow water or other liquids to accumulate on them, as well as dirt, grease and other substances that act as lubricants. In addition, the area of ​​contact with the sole, in this case, is limited by the protruding edges of the surface, which also reduces slip resistance. This factor must be taken into account when choosing tiles.

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According to the DIN 51097 method, in rooms where floors are often wet and where people walk on them barefoot (for example, swimming pool sides, children's pools, common shower rooms, saunas, etc.), the classification contains groups: A; B (A+B); C (A+B+C). Where A is the slipperiest tile.

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Friction coefficient is a parameter characterizing the degree of surface sliding. It is proportional to the force parallel to the interaction surface that must be applied in order to create relative motion between two bodies. The higher its characteristics such as smoothness and shine, the lower the coefficient of friction for floor surfaces, since this contributes to the appearance of a thin, continuous layer of water (as well as grease, dirt, etc.), which acts as a lubricant between the sole and the floor. Ceramic tiles, while smooth and shiny, create a slippery surface and increase the risk of falls and accidents.

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According to the DIN 51130 method, floors in production facilities or work areas where there is a high risk of slipping are classified into the following groups (according to the average inclination angle): NC; R9; R10; R11; R12; R13. Where R13 is the slipperiest tile.

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Material on this issue is presented in the article Slip resistance on dry and wet surfaces .

Question 3

Frost resistance - the ability of ceramic tiles to withstand freezing in a humid environment and at temperatures below 0 degrees Celsius. The freezing mechanism is divided into two stages. The first stage is the penetration of water from the environment into the pores of the tile. The second stage is the hardening (freezing) of water inside the pores. As is known, the transition of water from a liquid to a solid state is accompanied by an increase in volume, since the density of ice is less than the density of water. Thus, when water freezes inside the pores, the tile is subjected to mechanical stress, which can lead to cracks or chipping of part of the material.

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According to EN ISO 10545-12:1997, tests confirming frost resistance properties are not carried out as such. A material is considered frost-resistant if it falls into group 1 of materials according to the degree of water absorption (<3%).

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Based on the mechanisms described above, the frost resistance of a material is determined by the possibility of water penetration into the material, in other words, the degree of water absorption. Thus, if a material does not absorb water, it is frost-resistant, but if it does, it is not.

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Frost resistance also prevents ice from forming on the face of the tile. This is due to the fact that water, without getting inside the material through the pores of the top layer, seems to “roll off” from the surface.

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According to EN ISO 10545-12:1997, tests confirming frost resistance properties are carried out as follows: ceramic tiles or slabs, after being saturated with water, are subjected to alternate temperatures of +5 ° C and minus 5 ° C. They are then completely frozen for at least 100 freeze-thaw cycles. After 100 freeze/thaw cycles, the faces and edges of ceramic tiles or slabs are examined for damage.

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Based on the mechanisms described above, the frost resistance of a material is determined by two parameters:
1) The presence and number of pores that allow water to penetrate into the material;
2) The shape and size of the pores, the volume of voids of which, allows you to distribute the loads of the changing state of water.
It follows from this that frost resistance is directly related to water absorption: the lower the water absorption, the greater the likelihood that the material is frost-resistant. However, there are also highly porous materials (with a high rate of water absorption) that are characterized by frost resistance. Frost resistance in this case is due to the shape and size of the pores, allowing moisture to penetrate into the material without destroying it as a result of hydrothermal loads.

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The frost resistance property of ceramic tiles is not guaranteed in extremely low temperature zones (below -40 °C). This is due to the test conditions of EN ISO 10545-12:1997, as they are carried out at temperatures between +5°C and -5°C. In this regard, manufacturers mark materials suitable for use in such an environment with a special EXTRA°C sign, which in turn indicates testing in the temperature range from -50 °C to +100 °C.

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Material on this issue is presented in the article Frost resistance .

Question 4

Abrasion resistance is a mechanical characteristic of a lined surface. Indicates the surface’s resistance to wear due to exposure to rubbing objects, surfaces, and materials. Which expressions do you think are correct?

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The wear resistance requirements for unglazed ceramic tiles and slabs are set by EN 14411 and depend on water absorption and the method of their manufacture.

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Abrasion resistance is a property characteristic only of glazed ceramic tiles. Since intense and prolonged exposure to the surface over time can lead to partial loss of the glazed layer, and this, in turn, will lead to exposure of the ceramic mass and, as a consequence, to the loss of not only the aesthetic, but also the functional qualities of the facing surface. Damage to unglazed tiles is almost invisible, since abrasion of the top layer leads to exposure of the ceramic mass, which in unglazed tiles is no different from the top layer.

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Abrasion resistance also affects other functional characteristics of the ceramic tile surface, such as chemical and stain resistance and ease of maintenance. Naturally, this aspect is equally important for glazed and unglazed tiles, because... abrasion leads to a weakening of the tile structure itself, the appearance of pores and microcracks invisible to the naked eye, into which dirt, etc. gets clogged.

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According to the test method EN ISO 10545-7:1998, glazed tiles are divided into wear resistance classes, from "0" to "5". Where fifth class tiles are least resistant to abrasion.

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The important point is that unlike other quality tests on tiles, durability testing does not determine the value of the tile. The results of the study divide the tiles into classes, each of which corresponds to a specific purpose of the tile, and in no way to divide the tiles into “bad” and “good”.

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Information on this issue is presented in the article Abrasion resistance, wear resistance .

Question 5

The surface hardness of ceramic tiles is the ability of the cladding surface to withstand the mechanical stress of other materials. For ceramic facing materials or natural stones, this property is usually indicated in accordance with the mineralogical scale of hardness, the so-called Mohs scale, named after the German mineralogist Friedrich Mohs, who proposed his test method in 1811. Please indicate the correct statements in your opinion.

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Mohs scale - determined by which of ten standard minerals scratches the material being tested, and which of ten standard minerals scratches the material being tested.

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The Mohs scale (mineralogical hardness scale) is a set of reference minerals for determining relative hardness using the scratching method. 10 minerals, arranged in order of increasing hardness, were taken as standards.

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Glazed ceramic tiles are relatively hard, and scratches affect the aesthetic properties of the cladding, while also damaging its functional qualities.

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The Mohs scale is a method of rough comparative assessment of the hardness of materials according to the “harder - softer” system, where the material being tested is scratched by a reference mineral and its surface hardness on the Mohs scale is lower, or it is scratched by a reference mineral and its hardness is higher. Thus, the values ​​of the Mohs scale can be considered indicators of the absolute hardness of minerals.

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Unglazed ceramic tiles are relatively hard, and scratches only affect the aesthetic properties of the cladding, without damaging its functional qualities.

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Material on this issue is presented in the article Surface hardness .

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