The term craquelure itself refers to the crevices and cracks that form on the surface of the glaze. The pattern of these cracks is often circular, although they may be scattered across the surface of the glaze. The reason for the appearance of craquelure is either a difference in the coefficient of thermal expansion of the shard and the glaze, or deformation of the tile due to the impact of mechanical load on it.
The test method for determining the resistance to cracking of glazes (craquelure) of ceramic tiles and slabs is given in the EN ISO 10545-18 standard. To determine the resistance to cracking of glazes, tiles and slabs are subjected to high pressure steam in an autoclave. Then the tiles and slabs, after applying the dye to the glazed surfaces, are examined for the presence of cracks in the glaze.
“Late craquelure” occurs under the influence of the external environment during operation. The reasons for its appearance are: thermal shock, insufficient drying of the cement base, excessive cement content in the layer, excessive thickness of the mortar layer.
When craquelure appears on polished ceramic tiles and slabs, the term "polished craquelure" is used.
Glazed tiles with an "immediate crackle effect" are not considered defective, although manufacturers sometimes deliberately create collections of tiles with a "craquelure effect" for aesthetic purposes.
This defect can appear immediately after the end of the production cycle (in this case they speak of “immediate craquelure”) or some time after laying the tiles (in this case they speak of “late craquelure”).
The material on this issue is presented in the article “ Resistance to craquelure ” and “ Cracking of craquelure glaze ”.
The quality and value of the cladding directly depend on the symmetry and uniformity of its individual components, i.e. individual tiles in relation to the quality of the surface and its dimensions. That is why, any dimensional differences and asymmetries of the tiles, deviations of the surface from flatness, which violate the harmony of the cladding and worsen its appearance, will be considered defects. The quality of the surface is determined by the presence of the following defects: gaps, cracks, lack of glaze, unevenness, depressions, pits, damage to the vitrified surface, specks and stains, body defects, decorative defects, darkening, chipped edges and corners.
The method for controlling size and appearance characteristics is described in EN ISO 10545-2. To control the appearance, a minimum of 30 samples of tiles are selected, which must form a surface area of at least 1 m². The appearance of the tiles is checked visually (with the naked eye) at an illumination of 300 lux from a distance of 1 m from the observer’s eyes. According to the standard, preparation of the sample surface and visual assessment of the surface are carried out by different persons. Surface quality is expressed as a percentage of the number of tiles without defects.
If defective tiles do not exceed 5%, then the batch is assigned FIRST GRADE, and if they exceed 5%, then the batch is assigned SECOND GRADE.
The difference in size and dimensional deviations are expressed as a percentage of the working size of the tile.
The appearance characteristics, as well as the dimensional characteristics, are checked randomly on the tiles before they are packaged. Control is carried out visually by specially trained personnel (MANUAL SORTING) or by machine (AUTOMATIC SORTING).
The following type characteristics are important: length of the sides and thickness, straightness of the sides, orthogonality, flatness of the surface.
Information on this issue is presented in the article Dimensional and type characteristics .
Linear thermal expansion is expressed by dimensional changes in any material, including ceramics, due to changes in temperature. Almost all known materials expand as temperature increases and contract as temperature decreases. Moisture expansion refers to the expansion of the tile due to the absorption of moisture. The consequences of such swelling are similar to the expansion of tiles due to an increase in temperature (linear thermal expansion) and are due to the porous structure of the material.
The recommended upper limit for moisture expansion of ceramic tiles and slabs is 0.06% when testing according to ISO 10545-10 is applied. This means that the upper limit of moisture expansion of ceramic tiles and slabs should not exceed 6 mm/m.
A moisture expansion test is required for tiles with a water absorption value greater than 6%.
Methods for determining moisture expansion and temperature coefficient of linear expansion are given in the standards EN ISO 10545-10 and EN ISO 10545-8, respectively.
The coefficient of thermal expansion for floor and wall ceramic tiles varies from 4.1•10 -6 °C -1 to 8.1•10 -6 °C -1 . This means that elongation ranges from 40 to 80 thousandths of a millimeter per meter of ceramic tile and per degree rise in temperature.
The thermal coefficient of linear expansion α for ceramic tiles is calculated with an accuracy of 0.1•10 -6 °C -1 using the formula: α = dL/(L 0 •dT), where L 0 is the length of the test sample at room temperature; dL is the linear expansion of the test sample during the period of temperature change from room temperature to 100 °C; dT – temperature increase.
Material on this issue is presented in the article Linear thermal expansion and moisture expansion .
The surface hardness of ceramic tiles is the ability of the cladding surface to withstand the mechanical stress of other materials. For ceramic facing materials or natural stones, this property is usually indicated in accordance with the mineralogical scale of hardness, the so-called Mohs scale, named after the German mineralogist Friedrich Mohs, who proposed his test method in 1811. Please indicate the correct statements in your opinion.
Unglazed ceramic tiles are relatively hard, and scratches only affect the aesthetic properties of the cladding, without damaging its functional qualities.
The Mohs scale (mineralogical hardness scale) is a set of reference minerals for determining relative hardness using the scratching method. 10 minerals, arranged in order of increasing hardness, were taken as standards.
Glazed ceramic tiles are relatively hard, and scratches affect the aesthetic properties of the cladding, while also damaging its functional qualities.
The Mohs scale is a method of rough comparative assessment of the hardness of materials according to the “harder - softer” system, where the material being tested is scratched by a reference mineral and its surface hardness on the Mohs scale is lower, or it is scratched by a reference mineral and its hardness is higher. Thus, the values of the Mohs scale can be considered indicators of the absolute hardness of minerals.
Mohs scale - determined by which of ten standard minerals scratches the material being tested, and which of ten standard minerals scratches the material being tested.
Material on this issue is presented in the article Surface hardness .
Water absorption is a parameter that determines the porosity of ceramic tiles. It is measured by the amount of water that ceramic tiles absorb under certain laboratory conditions, and is expressed as a percentage of the dry weight of the tiles.
Mark the true statements.
The lower the degree of water absorption, the more resistant the tile will be to intense mechanical and hydrothermal influences.
According to EN ISO 10545-3, the penetration of water into the open pores of samples is determined using two methods: boiling and water saturation in a vacuum. When boiling, water saturation occurs only in easily filled open pores; with the vacuum method, almost all open pores are filled.
According to the EN 14411 standard, ceramic tiles and slabs are divided into three main groups based on water absorption. Where the third group corresponds to the lowest water absorption rates.
According to EN ISO 10545-3, the penetration of water into the open pores of samples is determined exclusively using the water saturation method in a vacuum. The boiling method, as a test that does not allow determining open porosity and bulk density, is considered obsolete.
A low water absorption coefficient indicates that the structure of the tile is porous, and a high coefficient indicates that the structure of the material is more dense.
Material on this issue is presented in the article Water absorption .
